Difference between revisions of "Facilities"

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<metadesc>Coherent X-ray Science Group facilities furnished by research grants awarded to Marcus Newton. </metadesc>
 
== Facilities: ==
 
== Facilities: ==
  
=== Synthesis Laboratory ===
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=== X-ray Diffraction Imaging Laboratory ===
  
 
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The X-ray Diffraction Imaging Facility consists of a Rigaku MicroMax-007 x-ray generator capable of focusing x-rays down to a spot size of 0.075 mm in diameter. X-ray are imaged with a Dectris Eiger2 area detector that is capable of single photon counting and can operate at high frequency.  A robotic diffractometer sample mounting stage permits automated and rapid measurement of multiple samples in sequence.  The system is capable of performing a wide variety of X-ray diffraction measurements on bulk samples, thin films and powders.  In addition, there is capacity for in-operando X-ray measurements coupled with laser, magnetic and electrical excitation.
  
The CXS Synthesis laboratory is primarily used for the synthesis of nanometre scale crystals and device structures.  Pulsed laser deposition (PLD) permits the synthesis of complex transition metal-oxide materials such as vanadates, cuprates and manganites as thin films or as heterostructures. Our laboratory houses a 248 nm KrF and a 193 nm ArF excimer laser, both of which are routinely used for pulsed laser deposition and laser-assisted fabrication. The CXS Synthesis laboratory is also equip with two thermal vacuum tube furnaces and various gases for nanoscale crystal synthesis via thermal CVD.  The synthesis equipment is supported by an optical table and accompanying overhead rack for electrical equipment.
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=== Sample Preparation Room ===
  
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The sample preparation room is equip with a fume cupboard that houses a spin coater, sonic bath, hot plate and weighing scale.  There is also an optical microscope with micromanipulator for sample inspection and manipulation.
  
=== X-ray Diffraction Laboratory ===
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=== Synthesis Laboratory ===
  
 
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The CXS X-ray diffraction laboratory houses two Rigaku microfocus rotating anode X-ray generators (Cu, Mo) housed in a single X-ray enclosure. This setup is ideally suited for nanoscale crystal structure determination and streamlined sample preparation for advanced lens-less X-ray imaging techniques such as Bragg Coherent X-ray Diffraction Imaging (BCXDI) as performed at synchrotron facilities such as the Diamond Light Source.
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The CXS Synthesis laboratory is primarily used for the synthesis of nanometre scale crystals and device structures.  Pulsed laser deposition (PLD) permits the synthesis of complex transition metal-oxide materials such as vanadates, cuprates and manganites as thin films or as heterostructures. Our laboratory houses a 248 nm KrF excimer laser for pulsed laser deposition and laser-assisted fabrication. The laboratory is also equip with two thermal vacuum tube furnaces and various gases for nanoscale crystal synthesis via thermal CVD.
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Latest revision as of 17:34, 14 November 2024



Facilities:

X-ray Diffraction Imaging Laboratory

Xrdi.jpg

The X-ray Diffraction Imaging Facility consists of a Rigaku MicroMax-007 x-ray generator capable of focusing x-rays down to a spot size of 0.075 mm in diameter. X-ray are imaged with a Dectris Eiger2 area detector that is capable of single photon counting and can operate at high frequency. A robotic diffractometer sample mounting stage permits automated and rapid measurement of multiple samples in sequence. The system is capable of performing a wide variety of X-ray diffraction measurements on bulk samples, thin films and powders. In addition, there is capacity for in-operando X-ray measurements coupled with laser, magnetic and electrical excitation.

Sample Preparation Room

Cleanroom.jpg

The sample preparation room is equip with a fume cupboard that houses a spin coater, sonic bath, hot plate and weighing scale. There is also an optical microscope with micromanipulator for sample inspection and manipulation.

Synthesis Laboratory

Laserlab.jpg


The CXS Synthesis laboratory is primarily used for the synthesis of nanometre scale crystals and device structures. Pulsed laser deposition (PLD) permits the synthesis of complex transition metal-oxide materials such as vanadates, cuprates and manganites as thin films or as heterostructures. Our laboratory houses a 248 nm KrF excimer laser for pulsed laser deposition and laser-assisted fabrication. The laboratory is also equip with two thermal vacuum tube furnaces and various gases for nanoscale crystal synthesis via thermal CVD.